Making Essential Oils: CO2's, Hydro Distillation and Absolutes Explained

>using a simple vacuum process, leaving only the
New methods of essential oil extraction are enteringessential oil behind. The use of solvents in the
the mainstream of aromatherapy, offering newextraction process notwithstanding, absolutes can
choices in oils never before available. With the newhave incredibly deep and complex aromas. The new
labels of 'CO2' and 'SCO2', along with the traditionalhigh tech distillation methods include: Carbon Dioxide
'steam' and 'hydro' distillations, 'absolutes', and 'coldand Supercritical Carbon Dioxide extraction. Both
pressing', a little education for the aromatherapymethods involve the use of carbon dioxide as the
enthusiast can go a long way in choosing the best'solvent' which carries the essential oil away from the
essential oil for your needs.raw plant material. The lower pressure CO2
Yes, even the age-old manufacture of pure essentialextraction involves chilling carbon dioxide to between
oils is going high-tech. New modern distillation methods35 and 55 degrees F, and pumping it through the
are entering the mainstream, offering wonderful newplant material at about 1000 psi. The carbon dioxide in
choices to aromatherapy enthusiasts and naturalthis condition is condensed to a liquid. Supercritical
health professionals. What are these new methods,CO2 extraction (SCO2) involves carbon dioxide
and more importantly, do they make better essentialheated to 87 degrees F and pumped through the
oils? More therapeutic? Nicer smelling? Well, for mostplant material at around 8,000 psi — under
varieties, the oils are simply ‘different' —these conditions, the carbon dioxide is likened to a
not necessarily ‘better'. For a few select oils,'dense fog' or vapor. With release of the pressure in
these new techniques MAY produce a more healingeither process, the carbon dioxide escapes in its
oil, and for others, the oils produced will truly add togaseous form, leaving the essential oil behind.
the palate of the natural perfumer. Here's a quickThese carbon dioxide methods have a couple of
look at all the major distillation methods in useadvantages: Like steam distillation, there are no
today…solvent residues left behind, and the resultant product
A number of factors determine the final quality of ais quite pure. Like solvent extraction, there is no heat
steam distilled essential oil. Aside from the plantapplied to the plant material or essential oil to alter it
material itself, most important are time, temperaturein any way. The oil produced is very accurate with
and pressure, and the quality of the distillationrespect to the original state of the plant. The CO2
equipment. Oils used in therapeutic aromatherapy aremethods also are the most efficient, producing the
really very chemically-intricate liquids; every oilmost oil per amount of plant (one of the reasons for
consists of many individual molecular componentsthe high cost of essential oils is the low yield of oil
which synergize to create the oil's overal biologicalfrom most plants — one ton of Rose petals
action and wonderful scent. Some of these moleculesproduces less than 1 pound of oil, for example). The
are fairly delicate structures which can be altered orefficiency of CO2 extraction is particularly important
destroyed by adverse environmental conditions. So,when rare or endangered plant species are involved,
much like a fine meal is more flavorful when madesuch as Indian Sandalwood oil — less of the
with patience, most oils benefit from a long, slowprecious plant is needed to produce an equivalent
'cooking' process.amount of oil.
The distillation vessel's temperature needs to beLast but not least is the expeller pressing of essential
carefully monitored and controlled so that the moreoils from the rinds of ripe fruits like lemons, limes,
delecate volitile compounds are preserved. The sameoranges and grapefruits. This method involves the
is true of the chamber's pressure. Lavender essentialsimple pressing of the rind at about 120 degrees F to
oil, for example, should not be processed at over 245extract the oil. Little, if any, alteration from the oil's
degrees F and three pounds per square inch oforiginal state occurs — these citrus oils retain
pressure (3 psi). Higher temperatures and/ortheir bright, fresh, uplifting aromas like that of smelling
pressures result in a 'harsh' aroma — morea wonderfully ripe fruit.
chemical than floral — and lessen the oil'sCO2's, with some obvious advantages, are not
therapeutic effects. In addition, the duration of thealways the best choice for a particular need. They still
distillation needs to be precisely monitored for each oilare the most expensive, despite their higher yields.
variety - not too long and not too short. This ensuresThe resultant product differs slightly compared to
all the important oil components are released, but theone produced another way — the oils
resultant oil is not 'overcooked', sometimes resultingproduced by steam distillation of some plants may
in an unpleasant 'medicinal' scent.sometimes be found to have a more agreeable
Despite the drawbacks of aggressive processing, higharoma. Patchouli oil, for example, seems to benefit
temperatures and pressures are often used tofrom the steam distillation process by becoming a
produces large quantities of oil in a short period oflittle warmer and richer. Many other essential oils are
time. These oils are usually destined for use inquite effectively produced via steam distillation, with
cosmetic and processed food manufacturing, but arelittle alteration from the original plant state. Some
sometimes sold to final consumers as essential oilsvarieties do very well with the new cold extraction
for use in aromatherapy. These oils will be lessmethods; the resin oils like Frankincense and Myrrh
expensive, but are of limited therapeutic value, andmay actually be more healing when made this way,
the difference is apparent when the aromas areand the oils of spices like Cardamom and Black
compared side-by-side. Some plants, and particularlyPepper can be more 'full bodied' in their scent. This
flowers, do not lend themselves to steam distilling.likely translates to greater therapeutic properties.
The volatile components are often too fragile, or tooProducing essential oils of aroma-therapeutic grade is
difficult to extract using other means. These oils willskill requiring years of experience. Making an equisite
be produced as 'absolutes' — and while notessential oil of any variety demands experience and
technically considered essential oils they can still be ofknow-how at every step of the way, from growing
therapeutic value. Jasmine oil and Rose oil in particularand harvesting the plant material to closely monitoring
are delicate flowers who's oils are often found inthe distillation itself. The making of a fine essential oil
'absolute' form.relies far more on knowledge and experience than it
The processing of an absolute first involves thedoes on the particular extraction method. There are,
hydrocarbon solvent extraction of a 'concrete' fromhowever, legitimate reasons to select one distillation
the plant material, a semi-solid mixture of typicallymethod over another — some plants simply
50% wax and 50% volatile oil. The concrete is againrequire a particular process to produce a fine oil, and
processed using ethyl alcohol (the same alcohol foundthe oil needed for a particular application may only be
in beer, wine, etc.) in which the wax is only slightlymade by one process. In the end, as is often the
soluble. The volatile plant oil separates into the alcoholcase in aromatherapy, your own sense of smell can
and this mixture is removed. The solvent is removedtell you which oil will work best for you.